nanomagnetite-fe3o4 as a highly efficient, green and recyclable catalyst for the synthesis of 4,4´-(arylmethylene)-bis(3-methyl-1-phenyl-1h-pyrazol-5-ol)s

Authors

abdolkarim zare

fereshteh abi

vahid khakyzadeh

ahmad reza moosavi-zare

alireza hasaninejad

abstract

nanomagnetite-fe3o4 is used as a highly efficient, mild, green and recyclable nanomagnetite catalyst for the synthesis of 4,4´-(arylmethylene)-bis(3-methyl-1-phenyl-1h-pyrazol-5-ol) derivatives in solvent-free conditions. the condensation reaction of 3-methyl-1-phenyl-1h-pyrazol-5(4h)-one with aromatic aldehydes affords the title compounds in high yields and short reaction times. the nanocatalyst is reusable for seven times without significant loss of its catalytic activity. short reaction times, high yields, generality, efficiency, recyclability of the catalyst for seven times, simple purification, clean reaction, and agreement with the green chemistry protocols are some advantages of in this method. the catalyst was characterized by transmission electron microscopy (tem), fourier transform infrared spectroscopy (ft-ir), x-ray diffractometer (xrd) and vibrating sample magnetometer (vsm).

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Journal title:

iranian journal of catalysis

Publisher: islamic azad university, shahreza branch

ISSN 2252-0236

volume 5

issue 4 2015

Keywords

[ ' n a n o m a g n e t i t e ' , ' f e 3 o 4 ' , ' n a n o m a g n e t i t e ' , 4 , ' 4 ´ ' , ' ( a r y l m e t h y l e n e ) ' , ' b i s ( 3 ' , ' m e t h y l ' , 1 , ' p h e n y l ' , ' 1 h ' , ' p y r a z o l ' , 5 , ' o l ) ' , 3 , ' m e t h y l ' , 1 , ' p h e n y l ' , ' 1 h ' , ' p y r a z o l ' , ' 5 ( 4 h ) ' , ' o n e ' , ' a r o m a t i c a l d e h y d e ' ]

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